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Abstract:	Die Kryotransfer-Rasterelektronenmikroskopie wird mittlerweile sehr häufig zur Erforschung von Abbindereaktionen in Zementen und anderen Baustoffen eingesetzt und kann heute als Standardverfahren angesehen werden. Ein wesentliches Interesse für industrielle Anwendungen besteht unter anderem darin, Untersuchungen des Zementleims in-situ bereits ab der Wasserzugabe bzw. ab der ersten Minute der Hydratation in so genannten “Zeitschnitten” durchzuführen. In der vorliegenden Arbeit wird der Einsatz eines Kryotransfer-Systems bei der Untersuchung der Abbindereaktionen des Zements in einem herkömmlichen Beton aufgezeigt. Als unterschiedliche Parameter wurden modellhaft Abbindezeiten von 1 Minute, 5 und 60 Minuten bei Abbindetemperaturen von 4 °C, 22 °C und 40 °C gewählt. Hydraulic Reactions of Cement in Mortar at Different Parameters Analytical Observations by Means of Cryo-Transfer-Scanning-Electron-Microscopy For the investigation of hydraulic reactions of cements and other building materials the cryo-transfer scanning-electron-microscopy is frequently used by now. Today the cryo-transfer technique is considered as a reference procedure. An essential concern in industrial applications is - amongst others - the insitu investigation of the cement paste at the very early state of hydration - just after the addition of water, respectively during the first minutes within so-called “time-cuts”. The present work illustrates the application of a cryo-transfer system for the investigations on hydraulic reactions of conventional concrete. Exemplary parameters were curing times of 1 minute, 5 and 60 minutes at curing temperatures of 4 °C, 22 °C and 40 °C.
Source:	Beton- und Stahlbetonbau 105 (2010), No. 8
Page/s:	521-528
Language of Publication:	German

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